Guinea Fowl

Only way I know how is to listen to them. The males make a single sound call, sort of 'ack ack ack'

the females make a double call, ack ACK ack ACK ack ACK.

the problem you'll have is with the 3 pearls, remembering which one is which unless you band them, or if they each have very different head markings, etc.

Good luck,
 
Like the others said, the easiest way to sex them is by their different calls. Just in case you've never heard the female's call, here it is:
 

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