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No higher order life forms in this world live without something else dying. Not emotionally pleasant, but that's reality.

I don't know what the laws are in FL, but the OP should be mum about whatever he decides to do. In other words, don't document what you do online.

Can you make some recommendations?

I think ethics are about as useful as tits on a boar hog. You know some people think raising chickens is unethical.

If anyone does release a raccoon (or any other creature) make sure the trap opening is pointed towards an open area. Don't do like I did once and set the trap opening in front of some large rocks. The coon felt trapped and freaked. Scared the living shirt out of me. The next time I caught a coon...

Just in case you have a diesel, it won't work.

For that matter he could buy dry ice at the grocery store and put it in an airtight enclosure. Not too airtight, though, or it will explode.

CO in car exhaust is lethal to animals much larger than raccoons. Humans die from it all of the time.

There's not enough CO2 in car exhaust to kill him, but there's definitely enough CO (carbon monoxide). That would be the most humane (like going to sleep).